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Substitution of 2-alkylidene-7-diethylaminobenzopirane: Crystal and molecular structure of 4-methyl-7-diethylamino-2-(5,5-dimethylcyclohexa-1,3-dione-2-iliden)-2H-1-benzopirane

โœ Scribed by D. S. Yufit; Yu. T. Struchkov; M. A. Kirpichenok; S. K. Gorozhankin; I. I. Grandberg

Publisher
SP MAIK Nauka/Interperiodica
Year
1991
Tongue
English
Weight
266 KB
Volume
31
Category
Article
ISSN
0022-4766

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โœ Anthony G. Borel; Frank S. Abbott ๐Ÿ“‚ Article ๐Ÿ“… 1990 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 452 KB

## Abstract Pentadeuteriophenyl clobazam 5 was synthesized in essentially quantitative isotopic purity, and characterized by ^1^Hโ€NMR and mass spectroscopy. The title compound was found to be โ‰ฅ98% pure by HPLC, and its retention time (t~R~ 6.17 min) was less than that of an authentic clobazam stand