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Substituted methyl 5β-cholan-24-oates II. 13C NMR spectral assignment

✍ Scribed by Kari Lappalainen; Erkki Kolehmainen; Mari Kaartinen; Reijo Kauppinen; Raimo Seppälä; Virpi Vatanen

Publisher
John Wiley and Sons
Year
1994
Tongue
English
Weight
266 KB
Volume
32
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

The ^13^C NMR spectra were recorded and assigned for nine derivatives of methyl 5β‐cholan‐24‐oates (esters of bile acids) including hydroxy, oxo and/or acetyloxy groups. Assignments were based on the empirical substituent‐induced chemical shifts (SCS), spectral comparison with compounds of similar structure, distortionless enhancement by polarization transfer (DEPT) and proton coupled ^13^C NMR measurements.

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