✦ LIBER ✦

Study on the feasibility of coupling large-volume injection to fast gas chromatography with mass spectrometric detection for analysis of organochlorine pesticides

✍ Scribed by Eva Korenková; Eva Matisová; Jaroslav Slobodník

Publisher: John Wiley and Sons
Year: 2003
Tongue: English
Weight: 163 KB
Volume: 26
Category: Article
ISSN: 1615-9306
DOI: 10.1002/jssc.200301269

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✦ Synopsis

Abstract

A combined use of programmable temperature vaporisation injector, fast oven temperature ramp, 0.1 mm ID analytical column and hydrogen carrier gas enabled injection of up to 20 μL of extract containing 15 organochlorine pesticides and separation of all analytes in less than 8 minutes.

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## Abstract This study describes an SPE coupled with large volume injection (LVI) analytical method for the analysis of organochlorine pesticides, BHC (α, β, Δ), aldrin, endosulfan (α, β), endrin, dieldrin, and DDT, from aqueous samples. Determination was carried out by GC with MS. The LODs of orga