Poly(methyl methacrylate)-silica hybrid materials (PMMA-SiO 2 ) were prepared by in situ polycondensation of alkoxysilane in the presence of trialkoxysilanefunctional PMMA. Infrared, differential scanning calorimetry, 29 Si and 13 C nuclear magnetic resonance spectroscopy, and thermogravimetric anal
Study of poly(methyl methacrylate–maleic anhydride)/silica hybrid materials
✍ Scribed by Tingxiu Xie; Chongguang Zhou; Shengyu Feng; Xinqiang Wang
- Publisher
- John Wiley and Sons
- Year
- 2000
- Tongue
- English
- Weight
- 144 KB
- Volume
- 75
- Category
- Article
- ISSN
- 0021-8995
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✦ Synopsis
Poly(methyl methacrylate-maleic anhydride) [P(MMA-MAn)] with active groups, anhydrides, was synthesized by radical copolymerization. Using P(MMA-MAn) as a basic polymer, the P(MMA-MAn)/SiO 2 hybrid materials were obtained by a sol-gel process in different ways. The structures of the materials were characterized by IR spectra, and their properties were studied by thermogravimetric analysis (TGA), dynamic mechanical analysis (DMA), and dynamic analysis (DA). The results show that the hybrids prepared in different ways have different properties, and the contents of SiO 2 also have influence on the properties of the hybrids.
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