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Studies toward the total synthesis of azaspiracids: synthesis of the FGHI ring domain

โœ Scribed by Makoto Sasaki; Yuko Iwamuro; Jyunichi Nemoto; Masato Oikawa

Book ID
104254167
Publisher
Elsevier Science
Year
2003
Tongue
French
Weight
283 KB
Volume
44
Category
Article
ISSN
0040-4039

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โœฆ Synopsis

Synthesis of the FGHI ring domain of azaspiracids, the causative agents for a new type of shellfish poisoning, azaspiracid poisoning (AZP), has been achieved. The synthesis features dithiane anion-epoxide coupling for convergent fragment assembly.

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Scheme 1. Structure of azaspiracid (1) and retrosynthetic analysis leading to FGHI ring framework 3 via key intermediate 2. previously known agents of diarrhetic shellfish poisoning. [1] This seasonally occurring toxin displays an unusually complex molecular assembly ยฑ it harbors a total of nine ri

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