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Studies on the diastereoselectivity of samarium(II) iodide mediated reductive carbocyclizations of ω-iodo-α,β-unsaturated esters prepared from 2-deoxy-d-ribose

✍ Scribed by Sharon M. Bennett; Raphinos Kouya Biboutou; Bita Samim Firouz Salari

Book ID
108387022
Publisher
Elsevier Science
Year
1998
Tongue
French
Weight
231 KB
Volume
39
Category
Article
ISSN
0040-4039

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✍ Bita Samim Firouz Salari; Raphinos Kouya Biboutou; Sharon M Bennett 📂 Article 📅 2000 🏛 Elsevier Science 🌐 French ⚖ 319 KB

Iodo-a,b-unsaturated esters were reduced with SmI 2 or Bu 3 SnH under different conditions to give carbocyclic compounds in good yield. The stereoselectivity of the SmI 2 cyclizations varies with the choice of promoter, the reaction temperature, the identity of the hydroxyl protecting groups and the

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