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Studies on the BF3·Et2O catalyzed Baeyer–Villiger reaction of spiroketalic steroidal ketones

✍ Scribed by Mariana Macias-Alonso; Jacek W. Morzycki; Martin A. Iglesias-Arteaga

Book ID
116892556
Publisher
Elsevier Science
Year
2011
Tongue
English
Weight
524 KB
Volume
76
Category
Article
ISSN
0039-128X

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✍ S. N. CRANE; D. J. BURNELL 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 42 KB 👁 1 views

The BF 3 •Et 2 O-Catalyzed Reaction of 1,2-Bis[(trimethylsilyl)oxy]cyclobutene and Analogues with Aromatic Ketones. -Aromatic ketones (I) and (V) undergo geminal acylation with cyclobutene (II) and its methylated analogues (VIII). Subsequent rearrangement, especially during aqueous work-up, results