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Studies in the Phenanthrene Series. VIII. Amino Alcohols Derived from 1,2,3,4,5,6,7,8-Octahydrophenanthrene 1

✍ Scribed by Kamp, Jacob van de; Mosettig, Erich

Book ID
127256971
Publisher
American Chemical Society
Year
1935
Tongue
English
Weight
352 KB
Volume
57
Category
Article
ISSN
0002-7863

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## Abstract Cyclization of ethyl (__E__)/(__Z__)‐[2‐(1‐cyclohexen‐1‐yl)cyclohexylidene]cyanoacetate (2) in cold concentrated sulfuric acid affords 10‐amino‐1,2,3,4,5,6,7,8‐octahydrophenanthrene‐9‐carboxylic acid (4) and 3,5,6,7,8,8a‐hexahydro‐3‐oxospiro‐[1__H__‐2‐benzopyran‐1,1′‐cyclohexane]‐4‐carb