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Structures of two niobium(IV) complexes: [N(C2H5)4]2[NbCl6] and [P(CH3)2(C6H5)H][NbCl5{P(CH3)2(C6H5)}]

✍ Scribed by Cotton, F. A. ;Diebold, M. P. ;Roth, W. J.

Book ID
114507175
Publisher
International Union of Crystallography
Year
1990
Tongue
English
Weight
416 KB
Volume
46
Category
Article
ISSN
0108-2701

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## CeH5CHzCsH4)2GdCl.THF]2 (1) and ( C ~H ~C H Z C ~H ~) ~E ~C I . T H F (2) were prepared by the reaction of LnC13 ( Ln=Gd, Er) with benzylcyclopentadienyl sodium in THF and characterized by elemental analysis, IR, 'H NMR, 13C NMR, MS and thermal gravimetry. The crystal structures of both compoun