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Structures of tetracarbonyl(2–3-η-maleic acid)iron, cis-[Fe(C4H4O4)(CO)4] (1) and tetracarbonyl(2–3-η-fumaric acid)iron, trans-[Fe(C4H4O4)(CO)4] (2)

✍ Scribed by Hsiou, Y. ;Wang, Y. ;Liu, L.-K.

Book ID: 114506085
Publisher: International Union of Crystallography
Year: 1989
Tongue: English
Weight: 420 KB
Volume: 45
Category: Article
ISSN: 0108-2701
DOI: 10.1107/s0108270188013368

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Section 3: Compound 4 [4] (80 mg, 0.075 mmol) and KC 8 (22 mg, 0.163 mmol) were placed in a reaction tube with a magnetic stirrer. Oxygen-free, dry THF (2 mL) was introduced into the reaction tube by vacuum transfer, and the reaction mixture was stirred at room temperature to produce a yellow soluti