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Structures of molecular addition compounds. IV. Trimethylamine–boron trifluoride, (H3C)3N–BF3

✍ Scribed by Geller, S. ;Hoard, J. L.

Book ID
114515702
Publisher
International Union of Crystallography
Year
1951
Tongue
English
Weight
882 KB
Volume
4
Category
Article
ISSN
0365-110X

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Trimethylamine-bis(trifluoromethyl) boranes R(CF 3 ) 2 B ´NMe 3 (R = cis/trans-CF 3 CF=CF (1/2), HCºC (3), H 2 C=CH (4), C 2 H 5 (5), C 6 H 5 CH 2 (6), C 6 F 5 (7), C 6 H 5 (8)) react with NEt 3 ´3 HF depending on the nature of R at 155±200 °C under replacement of the trimethylamine ligand to form