## Abstract Compound [(dph‐BIAN)Mg(THF)]~2~ (**2**) was prepared by reacting magnesium metal with 1,2‐bis[(2‐biphenyl)imino]acenaphthene (dph‐BIAN) in THF, followed by crystallization from toluene. Reaction of CaI~2~ with (dpp‐BIAN)Li~2~ in toluene afforded [(dpp‐BIAN)Li]~2~Ca (**3**) (dpp‐BIAN = 1
Structures of Alkali and Alkaline Earth Metal Clusters with Oxygen Donor Ligands
✍ Scribed by Katharina M. Fromm; Estelle D. Gueneau
- Publisher
- John Wiley and Sons
- Year
- 2004
- Weight
- 17 KB
- Volume
- 35
- Category
- Article
- ISSN
- 0931-7597
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## Abstract Compound [(dph‐BIAN)Mg(THF)]~2~(**2**) was prepared by reacting magnesium metal with 1,2‐ bis[(2‐biphenyl)imino]acenaphthene (dph‐BIAN) in THF, followed by crystallization from toluene. Reac‐ tion of CaI~2~ with (dpp‐BIAN)Li~2~ in toluene afforded [(dpp‐BIAN)Li]~2~Ca (**3**) (dpp‐BIAN =
## 17. XI. 89) The three ligands 1,4,7,1O-tetraazacyclododecane-1,4,7,1O-tetrakis(methylenephosphonic acid) (l), 1,4,7,1 Itetraazacyclotridecane-1,4,7,1 I-tetrakis(methy1enephosphonic acid) (Z), and 1,4,8,1 l-tetraazacyclotetradecane-1,4,8,1l-tetrakis(methylenephosphonic acid) (3) have been synthes