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Structures cristallines et moléculaires des muses macrocycliques. II. La trans-civettone et sa 2,4-dinitrophénylhydrazone

✍ Scribed by Gerald Bernardinelli; Raymond Gerdil


Publisher
John Wiley and Sons
Year
1982
Tongue
German
Weight
479 KB
Volume
65
Category
Article
ISSN
0018-019X

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✦ Synopsis


Crystal and Molecular Structure of Macrocyclic Musks.


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Structures cristallines et moléculaires
✍ Gérald Bernardinelli; Raymond Gerdil 📂 Article 📅 1982 🏛 John Wiley and Sons 🌐 German ⚖ 410 KB 👁 1 views

Crystal and Molecular Structure of Macrocyclic Musks. 111. Muscone and its 2,4-Dini trophenylhydrazone Summary Muscone (3-methylcyclopentadecanone C,,H,,O) forms orthorhombic plastic crystals with Z = 2 (a= 5.560 (4), b= 8.176 (6), c= 17.168 (20) A). Single crystals are obtained by zone melting at 2

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## Abstract The crystal structure of 5‐cyano‐4,4,6‐trimethyl‐2‐nitromethylene‐3‐oxo‐1,2,3,4‐tetrahydropyridine (compound I) and (Z)‐5‐(1‐acetoxy‐2‐nitroviny1)‐3,5‐dicyano‐4,4‐dimethyl‐2‐pyrazoline (compound II) has been determined by X‐ray diffraction analysis. The direct solution of the structures