Crystal and Molecular Structure of Macrocyclic Musks. 111. Muscone and its 2,4-Dini trophenylhydrazone Summary Muscone (3-methylcyclopentadecanone C,,H,,O) forms orthorhombic plastic crystals with Z = 2 (a= 5.560 (4), b= 8.176 (6), c= 17.168 (20) A). Single crystals are obtained by zone melting at 2
✦ LIBER ✦
Structures cristallines et moléculaires des muses macrocycliques. II. La trans-civettone et sa 2,4-dinitrophénylhydrazone
✍ Scribed by Gerald Bernardinelli; Raymond Gerdil
- Publisher
- John Wiley and Sons
- Year
- 1982
- Tongue
- German
- Weight
- 479 KB
- Volume
- 65
- Category
- Article
- ISSN
- 0018-019X
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✦ Synopsis
Crystal and Molecular Structure of Macrocyclic Musks.
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## Abstract The crystal structure of 5‐cyano‐4,4,6‐trimethyl‐2‐nitromethylene‐3‐oxo‐1,2,3,4‐tetrahydropyridine (compound I) and (Z)‐5‐(1‐acetoxy‐2‐nitroviny1)‐3,5‐dicyano‐4,4‐dimethyl‐2‐pyrazoline (compound II) has been determined by X‐ray diffraction analysis. The direct solution of the structures