Structure, thermal behavior, and IR investigation of bis(3-amino-1,2,4-triazolium)monohydrogen monophosphate
✍ Scribed by Leïla Baouab; Taha Guerfel; Monia Soussi; Amor Jouini
- Book ID
- 110320736
- Publisher
- Springer
- Year
- 2000
- Tongue
- English
- Weight
- 81 KB
- Volume
- 30
- Category
- Article
- ISSN
- 1572-8854
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The synthesis method, crystal structure determination, phase transitions studied by thermal analysis and IR spectrometric investigation of 2C 6 H 9 N 2 + .SO 4 2-are reported. The compound crystallizes in the monoclinic space group C2/c (no. 15) with a = 10.5068(4) Å, b = 10.2225(5) Å, c = 14.0422(7
Quarternary salts based upon 3-alkyl substituted 1-amino-1,2,3-triazolium cations (alkyl = methyl, ethyl, n-propyl, 2-propenyl, and n-butyl) have been synthesized and characterized by vibrational spectra, multinuclear NMR, elemental analysis, and DSC studies. Subsequent diazotization of these salts