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Structure of all-trans-3,4-didehydroretinal (retinal2)

โœ Scribed by Simmons, C. J. ;Asato, A. E. ;Liu, R. S. H.

Book ID
114503750
Publisher
International Union of Crystallography
Year
1986
Tongue
English
Weight
591 KB
Volume
42
Category
Article
ISSN
0108-2701

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## Abstract transโ€Ionylideneacetaldehydeโ€1โ€^3^H (3) was obtained by reduction of unlabeled aldehyde 1 with lithium borotritide, followed by reoxidation of the tritio alcohol 2. Condensation of aldehyde 3 with diethyl 3โ€cyanoโ€2โ€methylpropโ€2โ€enylphosphonate (7) afforded retinonitrileโ€11โ€^3^H (8) whic