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Structure of a new isobenzofuranone derivative from Nigella sativa Linn

✍ Scribed by B. S. Joshi; K. L. Singh; Raja Roy

Publisher
John Wiley and Sons
Year
2001
Tongue
English
Weight
80 KB
Volume
39
Category
Article
ISSN
0749-1581

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✦ Synopsis

Abstract

The seeds of Nigella sativa Linn contain a new isobenzofuranone derivative, 5‐hydroxy‐2,2‐dimethyl‐2,8‐dihydro‐6__H__‐furo[3,4‐g]chromen‐6‐one (1), obtained from the CHCl~3~ extract. Complete ^1^H and ^13^C assignments of the compound were carried out using one‐dimensional steady‐state difference NOE together with HMQC and HMBC experiments. Copyright © 2001 John Wiley & Sons, Ltd.

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## Communications DMF seems to be the solvent of choice, as DMF with cesium carbonate gave the highest overall yields.['] The success of the use of other group-I metal ions as templates shows a great variation with the metal ion.[g1