𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Structure of 5-(2-hydroxyethoxy)-6-[1-(4-methoxyphenyl)ethyl]-1,3-benzodioxole

✍ Scribed by Sicheri, F. V. ;Derry, W. B. ;Gupta, R. S. ;Yang, D. S. C.

Book ID
114509287
Publisher
International Union of Crystallography
Year
1992
Tongue
English
Weight
328 KB
Volume
48
Category
Article
ISSN
0108-2701

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Ethyl 4-(4-hydroxy-3-methoxyphenyl)-6-me
Ethyl 4-(4-hydroxy-3-methoxyphenyl)-6-methyl-2-thioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
✍ Shang, Zhen-Hua ;Xiu, Yong ;Lin, Yan-Yan 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 741 KB

In the title compound, C 15 H 18 N 2 O 4 S, the packing is consolidated by an intra/intermolecular bifurcated O-HÁ Á Á(O,O) and intermolecular N-HÁ Á ÁS hydrogen bonds. The tetrahydropyrimidin-2-one ring is twisted. ## Related literature For background, see: Kappe (1993). ## Experimental Cryst

Ethyl 4-{5-[1-(hydroxy­meth­yl)ethyl­ami
Ethyl 4-{5-[1-(hydroxy­meth­yl)ethyl­amino­carbon­yl]-1,3-benzodioxol-4-yl}-7-meth­oxy-3-benzodioxole-5-carboxyl­ate
✍ Qi, Xiu-Xiang ;Suo, Ji-Shuan ;Wang, Li-Min ;Guo, Xiao-He ;Cheng, Sen-Xiang 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 213 KB

In the title compound, C~23~H~25~NO~10~, the five-membered rings adopt envelope conformations and the dihedral angle between the two benzene rings is 67.1 (7)°. The crystal structure is stabilized by intramolecular N—H...O and intermolecular O—H...O hydrogen-bond interactions.