Molecules of the title compound, C 24 H 26 N 4 , are linked by C-HÁ Á ÁN hydrogen bonds, forming a C(5) chain along the [010] direction. Neighboring chains are connected by four C-HÁ Á Á interactions, resulting in the formation of a threedimensional network.
Structure of 4-[4'-(dimethylamino)phenylazo]phenyl acrylate (1) and 4-[4'-(dimethylamino)phenylazo]phenyl methacrylate (2)
✍ Scribed by Meetsma, A. ;Boer, T. S. ;Haitjema, H. J. ;Tan, Y. Y.
- Book ID
- 114509663
- Publisher
- International Union of Crystallography
- Year
- 1993
- Tongue
- English
- Weight
- 574 KB
- Volume
- 49
- Category
- Article
- ISSN
- 0108-2701
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.005 A Ê Disorder in solvent or counterion R factor = 0.046 wR factor = 0.159 Data-to-parameter ratio = 15.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 24 H 23 ClN 4 , crystallizes in space group P1, with two crystallographically independent molecules in the asymmetric unit. In both molecules, the pyrrolidine ring adopts a half-chair conformation. The molecular packing in the crystal is stabilized by intermolecular CÐHÁ Á ÁN h