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Structure of 13-methyl-2,10-dioxatricyclo[4.4.4.01,6]tetradecane at 96 K

✍ Scribed by Brown, K. L. ;Down, G. J. ;Dunitz, J. D. ;Seiler, P.


Book ID
114528413
Publisher
International Union of Crystallography
Year
1982
Weight
523 KB
Volume
38
Category
Article
ISSN
0567-7408

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✍ Bruce Gaede; Rodger Henry; Steven A. Chamberlin πŸ“‚ Article πŸ“… 2000 πŸ› Journal of Heterocyclic Chemistry 🌐 English βš– 179 KB

## Abstract The tricyclic title compound, a symmetrical dispiro oxygen heterocycle, was isolated as a byproduct in the hydrogenation of furfuryl alcohol in the presence of hydrochloric acid. NMR studies and single crystal X‐ray analysis have established the relative stereochemistry of the two ketal