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Structure Modification on Quaternary Rare Earth Thiophosphates: NaYbP2S6, NaSmP2S6, and KSmP2S7

✍ Scribed by Eun-Young Goh; Eun-Jeong Kim; Sung-Jin Kim

Publisher
Elsevier Science
Year
2001
Tongue
English
Weight
993 KB
Volume
160
Category
Article
ISSN
0022-4596

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✦ Synopsis

x ) 6ux at 7503C. The structures were determined by the single-crystal X-ray di4raction technique. The air-sensitive darkred crystals of NaYbP 2 S 6 crystallize in the triclinic space group P-1 with a ‫؍‬ 6.8241(10) A > , b ‫؍‬ 7.0371(10) A > , c ‫؍‬ 9.107(2) A > , ‫؍‬ 87.17(2)3, ‫؍‬ 87.62(2)3, ‫؍‬ 88.30(2)3, and Z ‫؍‬ 2. The yellow plate crystals of NaSmP 2 S 6 crystallize in the monoclinic space group P2 1 /a with a ‫؍‬ 11.0717( 10) A > , b ‫؍‬ 7.2999(1) A > , c ‫؍‬ 11.579(3) A > , ‫؍‬ 111.30(2)3, and Z ‫؍‬ 4. The pale yellow plate crystals of KSmP 2 S 7 crystallize in the monoclinic space group P2 1 /a with a ‫؍‬ 8.981(2) A > , b ‫؍‬ 12.254(2) A > , c ‫؍‬ 9.609(1) A > , ‫؍‬ 90.27(2)3, and Z ‫؍‬ 4.

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