Structure elucidation of a potent mutagen from human feces
โ Scribed by Hirai, Nobuhiro; Kingston, David G. I.; Van Tassell, Roger L.; Wilkins, Tracy D.
- Book ID
- 126902262
- Publisher
- American Chemical Society
- Year
- 1982
- Tongue
- English
- Weight
- 306 KB
- Volume
- 104
- Category
- Article
- ISSN
- 0002-7863
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๐ SIMILAR VOLUMES
The structure of the benzoquinone antibiotic, lemonomycin (1), has been characterized using spectroscopic methods. The pyrrolidine substructure is new to this class, and the sugar moiety is encountered for the first time.
reflux for 20 h and allowed to cool, and the nearly quantitatively precipitated dicyclohexylurea was filtered off and washed with a small amount of dichloromethane. The combined organic phases were concentrated in vacuum and the residue was dissolved in ether. The ether solution was washed with NaHC