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Structure determination on a twinned crystal of cesium pentaborate tetrahydrate, Cs[B5O6(OH)4].2H2O

✍ Scribed by Behm, H.

Book ID
114502256
Publisher
International Union of Crystallography
Year
1984
Tongue
English
Weight
318 KB
Volume
40
Category
Article
ISSN
0108-2701

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The crystal structure of synthetic Cs 2 [B 4 O 5 (OH) 4 ]3H 2 O was determined from single-crystal X-ray diffraction data. The compound is monoclinic, space group P2 1 /c; the unit cell parameters are a‫)2(424.8؍‬ A s , b‫)3(873.11؍‬ A > , c‫)5(061.31؍‬ A > , ‫؍‬ 92.06(3)Β°; Z‫.4؍‬ The crystal struct

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Large single crystals of the polar, hydrated pentaborates Me[B 5 O 6 (OH) 4 ]β€’2H 2 O (Me = Rb, NH 4 ) were grown from aqueous solutions. The structure of NH 4 [B 5 O 6 (OH) 4 ]β€’2H 2 O was redetermined and proved to be orthorhombic (space group Aba2 (No. 41) with a = 11.3192(7) Γ…, b = 11.0261(8) Γ…, c