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Structure determination of monohydrated trifolin (kaempferol 3-O-β-D-galactopyranoside) from laboratory powder diffraction data

✍ Scribed by Iván da Silva; Jesús G. Díaz; Javier González-platas

Publisher
John Wiley and Sons
Year
2011
Tongue
English
Weight
327 KB
Volume
100
Category
Article
ISSN
0022-3549

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✦ Synopsis

The crystal structure of monohydrated trifolin (kaempferol 3-O-β-D-galactopyranoside) (an important biologically active compound, which was isolated from the aerial part of Consolida oliveriana) has been determined from conventional laboratory X-ray powder diffraction data. Variable counting time technique was used during measurement and crystal structure was solved by means of Monte Carlo algorithm. The final structure was achieved by Rietveld refinement using both constraints and restraints on interatomic bond lengths and angles.

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