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Structure Characterization of Functional Histidine Residues and Carbethoxylated Derivatives in Peptides and Proteins by Mass Spectrometry

✍ Scribed by Kalkum, Markus; Przybylski, Michael; Glocker, Michael O.

Book ID: 126141361
Publisher: American Chemical Society
Year: 1998
Tongue: English
Weight: 454 KB
Volume: 9
Category: Article
ISSN: 1043-1802
DOI: 10.1021/bc970162t

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## Abstract A general labelling method is presented which allows the determination of the number of guanidine groups (related to arginine and homoarginine in peptides and proteins) by means of mass spectrometry. It implies a guanidine‐selective derivatization step with 2,3‐butanedione and an arylbo