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Structure and stereochemistry of cyclobutatusin, a diterpenoid containing a four-membered ring

โœ Scribed by Wang, Andrew H. J.; Paul, Iain C.; Zelnik, Raymond; Lavie, David; Levy, Elie C.

Book ID
126149375
Publisher
American Chemical Society
Year
1974
Tongue
English
Weight
273 KB
Volume
96
Category
Article
ISSN
0002-7863

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1. For the preparation of N,N'-dimethylchloroformamidine hydrochloride see reference 111. 2. N,N'-Dimethylchloroformamidine hydrochloride is refluxed for five hours with PC15 (molar ratio 1:l) in cc14. The crude, slightly greenish product crystallizes out o n concentration of the reaction solution.