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Structure and conformation of polysaccharides by NMR spectroscopy

✍ Scribed by B. Casu


Book ID
103550325
Publisher
Elsevier Science
Year
1982
Tongue
English
Weight
367 KB
Volume
2
Category
Article
ISSN
0144-8617

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Two macrocyclic polyether isomers were obtained by radical cyclization of (E)-8-iodo-3,6-dioxaoctyl-3ethoxycarbonylpropenoate and separated by liquid-solid chromatography over silica gel. They were characterized, for the Ðrst time, by two-dimensional NMR ; notably, the HMBC experiment gave access to