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Structure-activity relationship in heparin: A synthetic pentasaccharide with high affinity for antithrombin III and eliciting high anti-factor Xa activity

✍ Scribed by J. Choay; M. Petitou; J.C. Lormeau; P. Sinaÿ; B. Casu; G. Gatti

Book ID: 115756522
Publisher: Elsevier Science
Year: 1983
Tongue: English
Weight: 504 KB
Volume: 116
Category: Article
ISSN: 0006-291X
DOI: 10.1016/0006-291x(83)90550-8

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Structure-activity relationship in hepar

Structure-activity relationship in heparin: A synthetic pentasaccharide with high affinity for antithrombin III and eliciting high anti-factor Xa activity

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The synthesis of tri-N-acetylated heparin pentasaccharide 2 is described. It was assembled from five suitably blocked monosaccharide units (S7). Glucuronic-acid building block 4 was prepared from glucose by direct Jones oxidation of the 6-0-trityl derivative 18. The resulting acid 16 was esterified