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Structural Study of Hydrated/Dehydrated Manganese Thiophene-2,5-diphosphonate Metal Organic Frameworks, Mn 2 (O 3 P–C 4 H 2 S–PO 3 )·2H 2 O

✍ Scribed by Rueff, Jean-Michel; Perez, Olivier; Pautrat, Alain; Barrier, Nicolas; Hix, Gary B.; Hernot, Sylvie; Couthon-Gourvès, Hélène; Jaffrès, Paul-Alain

Book ID
115478071
Publisher
American Chemical Society
Year
2012
Tongue
English
Weight
651 KB
Volume
51
Category
Article
ISSN
0020-1669

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Hydrothermal Synthesis, Powder Structural Determination, and Magnetic Study of the Novel Hydrated Iron Diphosphonate [Fe2(H2O)2(O3P–CH2–PO3H)2](H2O)2 or MIL-13
✍ M. Riou-Cavellec; C. Serre; J. Robino; M. Noguès; J.-M. Grenèche; G. Férey 📂 Article 📅 1999 🏛 Elsevier Science 🌐 English ⚖ 651 KB

Fe 2 (H 2 O) 2 (O 3 P+CH 2 +PO 3 H) 2 ](H 2 O) 2 or MIL-13 was prepared hydrothermally (120 h at 473 K). Its structure was determined by powder X-ray di4raction. This compound crystallizes in the triclinic system (P-1) with the following cell parameters: a ‫؍‬ 9.8487(6) A > , b ‫؍‬ 8.0308(5) A > , c