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Structural Study by Wide-Angle X-ray Scattering of the Spin Transition Molecular Materials [Fe(Htrz) 2 (trz)](BF 4 ) and [Fe(NH 2 trz) 3 ](NO 3 ) 2 (Htrz = 1,2,4-4 H -Triazole, trz = 1,2,4-Triazolato)

✍ Scribed by Verelst, Marc; Sommier, Line; Lecante, Pierre; Mosset, Alain; Kahn, Olivier

Book ID: 126452670
Publisher: American Chemical Society
Year: 1998
Tongue: English
Weight: 134 KB
Volume: 10
Category: Article
ISSN: 0897-4756
DOI: 10.1021/cm970375s

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## Abstract By changing the surfactant/water ratio, nanoparticles of the iron(II) spin crossover material, [Fe(NH~2~‐trz)~3~]Br~2~⋅3 H~2~O (with NH~2~‐trz=4‐amino‐1,2,4‐triazole), have been synthesised from 1 μm down to 30 nm (see figure). Magnetic and reflectivity experiments indicate that the cri