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Structural, Solid-State NMR and Theoretical Studies of the Inverse-Coordination of Lithium Chloride Using Group 13 Phosphide Hosts

✍ Scribed by Melinda J. Duer; Felipe García; Jonathan M. Goodman; Jörg P. Hehn; Richard A. Kowenicki; Vesal Naseri; Mary McPartlin; Matthew L. Stead; Robin Stein; Dominic S. Wright

Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
492 KB
Volume
13
Category
Article
ISSN
0947-6539

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13C CP/MAS NMR study of a phenyl group r
13C CP/MAS NMR study of a phenyl group rotation in the solid state using T1ρ, lineshape and 2D EXSY measurements
✍ Frank G. Riddell; Murray Bremner; John H. Strange 📂 Article 📅 1994 🏛 John Wiley and Sons 🌐 English ⚖ 316 KB

## Abstract A combination of solid‐state ^13^C CP/MAS NMR methods was used to study the rates of rotation of the phenyl group in 3,5‐dimethyl‐1‐phenylhex‐1‐yn‐3‐ol. The methods used were __T__~1ρ~ measurements, lineshape analysis and 2D exchange spectroscopy over the temperature range 219–284 K. Th