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Structural information from quadrupolar nuclei in solid state NMR

✍ Scribed by Sharon E. Ashbrook; Melinda J. Duer

Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
844 KB
Volume
28A
Category
Article
ISSN
1546-6086

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7Li solid-state NMR of lithium amides: s
7Li solid-state NMR of lithium amides: structural information from 7Li quadrupolar coupling constants
✍ Michael Hartung; Harald GΓΌnther; Jean-Paul Amoureux; Christian FernandΓ©z πŸ“‚ Article πŸ“… 1998 πŸ› John Wiley and Sons 🌐 English βš– 333 KB πŸ‘ 2 views

Lithium-7 quadrupolar coupling constants, s(7Li), were measured for a number of microcrystalline lithium amides by solid-state 7Li magic angle spinning (MAS) NMR. A linear correlation between s(7Li) and the structural NÈLiÈN angle known from x-ray di †raction work was found : s(7Li) \ (4.1 ^0.5) ‑ N