## Abstract The structure elucidations and complete ^1^H and ^13^C NMR assignments are reported for two new xanthone derivatives: 1,7‐dihydroxy‐2‐methoxy‐3‐(3‐methylbut‐2‐enyl)‐9__H__‐xanthen‐9‐one (1) and 1‐hydroxy‐4,7‐dimethoxy‐6‐(3‐oxobutyl)‐9__H__‐xanthen‐9‐one (2). Both of these secondary meta
Structural elucidation and NMR assignments of four aromatic lactones from a mangrove endophytic fungus (No. GX4-1B)
✍ Scribed by Hongbo Huang; Qing Li; Xiaojun Feng; Bin Chen; Jun Wang; Lan Liu; Zhigang She; Yongcheng Lin
- Publisher
- John Wiley and Sons
- Year
- 2010
- Tongue
- English
- Weight
- 94 KB
- Volume
- 48
- Category
- Article
- ISSN
- 0749-1581
- DOI
- 10.1002/mrc.2605
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✦ Synopsis
Abstract
Two new aromatic lactones, 6‐hydroxy‐4‐hydroxymethyl‐8‐methoxy‐3‐ methylisocoumarin (1) and 1,10‐dihydroxy‐8‐methyl‐dibenz[b, e]oxepin‐6,11‐dione (2), together with two known compounds, 1,10‐dihydroxy‐dibenz[b, e]oxepin‐6,11‐dione (3) and 3‐hydroxymethyl‐6,8‐dimethoxycoumarin (4), were isolated from a mangrove endophytic fungus (No. GX4‐1B) collected from the South China Sea. Their structures were elucidated and the data of ^1^H and ^13^C NMR were assigned completely by HREIMS, 1D and 2D NMR experiments including HMQC, HMBC and NOESY. Copyright © 2010 John Wiley & Sons, Ltd.
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