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Structural, Electrochemical and Spectroscopic Characterization of a Redox Pair of Sulfite-Based Polyoxotungstates: α-[W18O54(SO3)2] 4- and α-[W18O54(SO3)2] 5-.

✍ Scribed by Nigel Fay; Alan M. Bond; Carole Baffert; John F. Boas; John R. Pilbrow; De-Liang Long; Leroy Cronin

Publisher: John Wiley and Sons
Year: 2007
Weight: 15 KB
Volume: 38
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200729027

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✦ Synopsis

Abstract

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## Abstract The synthesis, isolation and structural characterization of the sulfite polyoxomolybdate clusters α‐(__D__~3__h__~)(C~20~H~44~N)~4~{α‐[Mo~18~O~54~(SO~3~)~2~]}⋅CH~3~CN and β‐(__D__~3__d__~)(C~20~H~44~N)~4~{β‐[Mo~18~O~54~(SO~3~)~2~]}⋅CH~3~CN is presented. Voltammetric studies in acetonitr