Structural determinations of some chloroazepine-2,5-diones using a lanthanide shift reagent
โ Scribed by D. Scott Wilbur
- Book ID
- 112127487
- Publisher
- Journal of Heterocyclic Chemistry
- Year
- 1984
- Tongue
- English
- Weight
- 436 KB
- Volume
- 21
- Category
- Article
- ISSN
- 0022-152X
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๐ SIMILAR VOLUMES
## Abstract The position of the lanthanide atom calculated from the pseudocontact shift equation was studied for 2โadamantanol and 2โmethylโ, 2โethylโ, 2โpropylโ, 2โbutylโ2โadamantanol. The possible methods of calculation considering rotation of the methyl group were ascertained in the case of 2โme
of the following in a volume of 1 liter: naphthalene (150 g), 2,5-diphenyloxazole (8 g), 1,4-bis(4-methyl-5-phenyl-oxazol-2-yI)benzene (0.6 g), ethylene glycol (20 ml), 2-ethoxyethanol(lOO ml), and toluene to make 1 liter. The radioactivity was measured in the liquid scintillation counter with an 18