Structural characterisation of nickel silicide performed by two-dimensional X-ray microdiffraction
β Scribed by P. Colombi; E. Bontempi; U.M. Meotto; S. Porro; C. Ricciardi; L. Scaltrito; S. Ferrero; G. Richieri; L. Merlin; L.E. Depero
- Publisher
- Elsevier Science
- Year
- 2004
- Tongue
- English
- Weight
- 341 KB
- Volume
- 114-115
- Category
- Article
- ISSN
- 0921-5107
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## Abstract A series of (Β±)β3βarylβ1βazabicyclo[2.2.2]octanβ3βols were synthesized and studied by ^1^H, ^13^C and 2D NMR spectroscopy, and the crystal structure of (Β±)β3β(4βmethylphenyl)β1βazabicyclo[2.2.2]octanβ3βol was determined by Xβray diffraction. The combined use of COSY, NOESY and ^1^Hβ^13^
EIVI Fig. 1. Cyclovoltammograins of 1 and 4. (---): Voltammogram of 1 embedded in a carbon paste electrode [12] in DMSO/O.l M Bu,NC10,, scan rate 1 mVs-', Ep(red) = -0.20, -0.46, -0.69 V; E,(ox) = -0.15, -0.41, -0.58 V. (--): Solution cyclic voltammogram of 4 in DMSO/O.I M Bu,NCIO, on a 0.07 cm2 Pt