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Structural and physical properties of a new organic superconductor, (BEDT-TTF)4Pd(CN)4H2O

✍ Scribed by Takehiko Mori; Kiyonori Kato; Yusei Maruyama; Hiroo Inokuchi; Hatsumi Mori; Izumi Hirabayashi; Shoji Tanaka

Publisher
Elsevier Science
Year
1992
Tongue
English
Weight
388 KB
Volume
82
Category
Article
ISSN
0038-1098

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Bromohexyl)-3¢,4¢-ethylenedioxy)-2,2¢-bithiophene (3): Into a roundbottomed flask were introduced EDOT (5.9 g, 41.4 mmol) and 150 mL of tetrahydrofuran (THF). The mixture was cooled to ±40 C and butyllithium, 2.5 M in hexanes (19 mL, 47.5 mmol), was added rapidly. After 1 h stirring, tributyltin chl