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Structural and optical selectivity of hydroxy ester hydrolysis by α-chymotrypsin

✍ Scribed by Iwao Tabushi; Hidenori Yamada; Haruhito Sato

Publisher
Elsevier Science
Year
1975
Tongue
French
Weight
183 KB
Volume
16
Category
Article
ISSN
0040-4039

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Preparation of optically active α-hydrox
Preparation of optically active α-hydroxy ketone derivatives by Enzyme-Mediated Hydrolysis of Enol Esters
✍ Kazutsugu Matsumoto; Natsuko Suzuki; Hiromichi Ohta 📂 Article 📅 1990 🏛 Elsevier Science 🌐 French ⚖ 257 KB

A new method of preparation of optically active a-hydroxy ketone derivatives has been developed. Incubation of (Z)-3-propionyloxy4-benzyloxy-2-pentcne (la) with lipasc OF gave optically pure (R)-cnol propionatc la, which in bun was converted without raccmization to @)-ketone 2a by the aid ofLiAlH4.