𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Striking different behavior in the activation of α-olefins by homogeneous and heterogenized catalysts based on η5-cyclopentadienyl nickel derivatives

✍ Scribed by A.M. Raspolli Galletti; G. Geri; G. Sbrana; M. Marchionna; P. Ferrarini


Book ID
103997710
Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
622 KB
Volume
111
Category
Article
ISSN
1381-1169

No coin nor oath required. For personal study only.

✦ Synopsis


Homogeneous

-q5-cyclopentadienyl nickel catalysts have been applied to ethylene oligomerization. Their activity, enhanced by the presence of Al(OEt)Et, as co-catalyst, resulted the highest up to now reported for this type of complexes. The same catalytic systems were also able to oligomerize propylene as well as ethylene/propylene mixtures. In particular propylene was converted into branched dimers, mostly 2,3_dimethylbutenes. Heterogenization of the above system, carried out by anchoring the nickel derivative to a styrene/divinylbenzene resin properly functionalized with the cyclopentadienyl group, caused a drastic change of the selectivity of the process, ethylene polymerization to HDPE taking place instead of oligomerization.