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Stopped flow Pulse-Fourier transform NMR. Observation of intermediates in the tricyanovinylation of N,N-dimethylaniline in methanol

✍ Scribed by M.J.T. Robinson; Stuart M. Rosenfeld

Publisher
Elsevier Science
Year
1975
Tongue
French
Weight
203 KB
Volume
16
Category
Article
ISSN
0040-4039

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Stopped-flow fourier-transform NMR and N
Stopped-flow fourier-transform NMR and NMR line broadening studies of the rates of dimethyl sulphoxide exchange with the hexakis(dimethylsulphoxide) complexes of aluminium(III), gallium(III) ions in nitromethane solution
✍ AndrΓ© E. Merbach; Peter Moore; Oliver W. Howarth; Colin H. McAteer πŸ“‚ Article πŸ“… 1980 πŸ› Elsevier Science 🌐 English βš– 685 KB

Stopped-flow Fourier-transform NMR and conventional NMR line broadening experiments have been used to determine rate data for dimethyl sulphoxide (DMSO) exchange with the [M(DMSO),] " ions (M = Al(III), Ga(III)) in nitromethane-d3 solution over a temperature range of 105 K (Al/III)) and 112 K (Ga-(I