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Steroidal Indoxyls, Indoles, and Quinolines 1

โœ Scribed by Hassner, Alfred; Haddadin, Makhluf J.; Catsoulacos, P.

Book ID
127023430
Publisher
American Chemical Society
Year
1966
Tongue
English
Weight
1017 KB
Volume
31
Category
Article
ISSN
0022-3263

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A novel synthesis of steroidal indoxyls
A novel synthesis of steroidal indoxyls and indoles
โœ Alfred Hassner; Makhluf J. Haddadin ๐Ÿ“‚ Article ๐Ÿ“… 1962 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 123 KB

IN attempts towards the synthesis of steroidal alkaloids1 we treated 5androstene-3B-ol-17-one with g-nitrobenzaldehyde in basic solution and obtained instead of the expected 16-(2-nitrobenzal) compound a yellow acidic product, m.p. 267-269' (dec.), in 75 per cent yield, to which structure Ia is attr