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Stereoselective synthesis of (±)-palitantin

✍ Scribed by Akitami Ichihara; Makoto Ubukata; Sadao Sakamura

Book ID
104235566
Publisher
Elsevier Science
Year
1977
Tongue
French
Weight
198 KB
Volume
18
Category
Article
ISSN
0040-4039

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Synthesis of (+)-palitantin
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Quit& acid was utilized fiir the synthesis of (+)-palitantin adopting the chlron approach. Perdnent methodology includes stereocontrolled free-radical deoxygenation, functional group adjustments and an a-keto hydmxymethylation teaction.

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+)-Palitantin (2) has been synthesized in 25% overall yield from the (5R)-tert-butyldimethylsiloxy-2cyclohexenone [(R)-I] where a remarkable diastereoselective cat. OsO4 cis-dihydroxylation of (R)-I furnished the precursor of the optically pure (5R,6R)-bis-trimethylsiloxy 2-cyclohexenone (7) which u

ChemInform Abstract: Asymmetric Synthesi
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✍ Georges Hareau; Masakazu Koiwa; Takeshi Hanazawa; Fumie Sato 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 25 KB 👁 1 views

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