𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Stereoselective Synthesis of 8-Aza-9,11-ethenoprostaglandin H1

✍ Scribed by Barco, Achille ;Benetti, Simonetta ;Baraldi, Pier Giovanni ;Moroder, Fabio ;Pollini, Gian Piero ;Simoni, Daniele

Publisher
John Wiley and Sons
Year
1982
Tongue
English
Weight
309 KB
Volume
1982
Category
Article
ISSN
0947-3440

No coin nor oath required. For personal study only.

✦ Synopsis

Abstract

A stereoselective synthesis of the title compound [8‐aza‐9,11‐etheno‐PGH~1~ (3)] starting from butyl 2‐(p‐tolylsulfonyl)‐2‐azabicyclo[2.2.1]hept‐5‐ene‐exo‐3‐carboxylate (5) is described.

📜 SIMILAR VOLUMES

Stereoselective synthesis of [11 β-3H]pr
Stereoselective synthesis of [11 β-3H]prostaglandin E1
✍ G. L. Bundy; J. A. Easter; L. S. Banitt; Y. Philopoulos; A. J. Wickrema Sinha; R 📂 Article 📅 1993 🏛 John Wiley and Sons 🌐 French ⚖ 533 KB

## Abstract This report describes an efficient stereoselective synthesis of [11β‐^3^H]prostaglandin E~1~ ([11β‐^3^H]PGE~1~). The key multiply protected 11‐keto intermediate was prepared in only three steps from PGE~1~. Reduction of the ketone function at C‐11 with sodium borodeuteride and sodium bo

ChemInform Abstract: Synthesis of 8-Subs
ChemInform Abstract: Synthesis of 8-Substituted 5H,9H-6-Oxa-7-aza-benzocyclononene-10,11-dione-11-O-methyloximes, a New [1,2]-Oxazonine Ring System.
✍ Alfons Pascual; Hugo Ziegler; Stephan Trah; Peter Ertl; Tammo Winkler 📂 Article 📅 2010 🏛 John Wiley and Sons ⚖ 34 KB 👁 1 views

## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a “Full Text” option. The original article is trackable v

Synthesis and anti-inflammatory activity
Synthesis and anti-inflammatory activity of 8H-1-thia-8-aza-dibenzo[e,h]azulenes
✍ Ivana Ozimec Landek; Dijana Pešić; Mladen Merćep; Barbara Stanić; Milan Mesić 📂 Article 📅 2011 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 162 KB

## Abstract Synthesis of a novel class of fused heterotetracyclic compounds, 8__H__‐1‐thia‐8‐aza‐dibenzo[__e__,__h__]azulenes (**VII**), is described. Starting __N__‐benzoyl‐protected 5__H__‐dibenzo[__b__,__f__]azepine (**XI**, PG = Bz) was oxidized to 5‐benzoyl‐10,11‐epoxy‐10,11‐dihydro‐5__H__‐dib

Assignment of the 1H and 13C NMR spectra
Assignment of the 1H and 13C NMR spectra of 9-deoxo-9a-aza-9a-homoerythromycin A, 9-deoxo-9a-aza-9a-homoerythromycin A 11,12-hydrogenborate and azithromycin 11,12-hydrogenborate
✍ Miguel Bayod-Jasanada; Rodrigo J. Carbajo; Fernando López-Ortiz 📂 Article 📅 1998 🏛 John Wiley and Sons 🌐 English ⚖ 276 KB 👁 1 views

The 1H and 13C NMR spectra of 9-deoxo-9a-aza-9a-homoerythromycin A, its 11,12-hydrogenborate derivative and azithromycin 11,12-hydrogenborate were unambiguously assigned using a combination of 1D and 2D HÈC correlation spectra.