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Stereoselective Nucleophilic Acylation of Benzaldehyde with a Crotonaldehyde-d1 Reagent

✍ Scribed by Priv.-Doz. Dr. Manfred Braun; Wilhelm Hild

Publisher: John Wiley and Sons
Year: 1984
Tongue: English
Weight: 225 KB
Volume: 23
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.198407231

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## Abstract The title compound **4** is generated from the phosphoric amide **5** in tetrahydrofuran with butyllithium. The lithium reagent **4** is stable at room temperature; its reactions with electrophiles furnish the products **6–22**, **26**, **27**, see __Table 1__ and the __Scheme__. A seco