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Stereodivergent Approach to β-Hydroxy α-Amino Acids from C 2 -Symmetrical Alk-2-yne-1,4-diols

✍ Scribed by Amador, Marta; Ariza, Xavier; Garcia, Jordi; Sevilla, Sara

Book ID: 120165153
Publisher: American Chemical Society
Year: 2002
Tongue: English
Weight: 92 KB
Volume: 4
Category: Article
ISSN: 1523-7060
DOI: 10.1021/ol0270428

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## Abstract Aldol reaction of 7‐chloro‐1,3‐dihydro‐1‐methyl‐5‐phenyl‐2__H__‐1,4‐benzodiazepin‐2‐one (**1**) with 4‐substituted __α__‐methylcinnamaldehydes **2**–**5** afforded a mixture of __threo__‐ and __erythro__‐3‐(3‐aryl‐1‐hydroxy‐2‐methylprop‐2‐enyl)‐7‐chloro‐1,3‐dihydro‐1‐methyl‐5‐phenyl‐2__