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Stereocontrolled synthesis of (+)-lycoperdic acid based on a palladium catalyzed reaction using a serine-derived organozinc reagent

✍ Scribed by Hidekazu Masaki; Tomoko Mizozoe; Tomoyuki Esumi; Yoshiharu Iwabuchi; Susumi Hatakeyama

Publisher: Elsevier Science
Year: 2000
Tongue: French
Weight: 147 KB
Volume: 41
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)00719-x

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✦ Synopsis

An ecient stereocontrolled synthesis of (+)-lycoperdic acid has been achieved based on palladium catalyzed cross-coupling reaction of (Z)-1-(tert-butyldimethylsiloxy)-3-iodo-6-(p-methoxybenzyl)oxy-2-hexene with the organozinc reagent, prepared from N-Boc-b-iodoalanine methyl ester.

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