𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Stereocontrolled synthesis of (7E,9Z)-[9,10-2H]-conjugated linoleic acid

✍ Scribed by Garance Broustal; Olivier Loreau


Publisher
John Wiley and Sons
Year
2004
Tongue
French
Weight
89 KB
Volume
47
Category
Article
ISSN
0022-2135

No coin nor oath required. For personal study only.

✦ Synopsis


Abstract

To study the metabolism of minor conjugated linoleic acid isomers (CLAs), (7E,9Z)‐[9,10‐^2^H] CLA was prepared in three steps from a conjugated enyne precursor. In the labelling step, deuterium atoms were introduced by partial reduction of the triple bond using deuterated disiamylborane and acetic acid‐d~4~. Deuterated (7E,9Z) CLA was obtained with high isotopic enrichment (>99%) and purity greater than 95%. Copyright Β© 2004 John Wiley & Sons, Ltd.


πŸ“œ SIMILAR VOLUMES


Synthesis of 9-Oxo- and 10-Hydroxy-2E-de
✍ G. Yu. Ishmuratov; R. Ya. Kharisov; O. V. Botsman; N. M. Ishmuratova; G. A. Tols πŸ“‚ Article πŸ“… 2003 πŸ› John Wiley and Sons βš– 50 KB πŸ‘ 1 views