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Stereochemistry of the stereoselective epoxidation and hydroboration of hexamethyl (Dewar benzene)

✍ Scribed by Leo A. Paquette; Stanley A. Lang Jr.; Michael R. Short; Bruce Parkinson; Jon Clardy

Publisher
Elsevier Science
Year
1972
Tongue
French
Weight
185 KB
Volume
13
Category
Article
ISSN
0040-4039

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## Abstract The reactions of 1‐azido‐2,4,6‐trimethyl‐ and 1‐azido‐2,6‐dimethylbenzene with hexamethyl‐__Dewar__‐benzene (HMDB) give rise to the pentamethyl(iminoethyl)‐4__H__‐1,2‐diazepines **4** and **5**, respectively. The X‐ray crystal‐structure analysis of **5** unequivocally established these