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Stereochemical studies of polyols from the polyene macrolide lienomycin

โœ Scribed by Pawlak, Jan; Nakanishi, Koji; Iwashita, Takashi; Borowski, Edward

Book ID
118062390
Publisher
American Chemical Society
Year
1987
Tongue
English
Weight
648 KB
Volume
52
Category
Article
ISSN
0022-3263

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The tetraformylal derivative of mycoticin A and B 2 has been prepared in high yield from the natural products 1. 2-D COSY NMR and NOEDS experiments allow assignment of all nonequivalent hydrogens in 2. NOE difference experiments shed light on the relative stereochemistry and conformation of the skip

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The degradation of prototype members of the skipped-polyol polyene macrolide class, mycoticins A and B, is reported. The characterization of the resultant fragments allows a partial structure determination to be achieved. The polyene macrolides comprise a large class of natural products which displ