Stability and purity of low-polarity adsorbents for coupled supercritical fluid extraction-supercritical fluid chromatography-flame ionization detection
✍ Scribed by U. Petersson; K.E. Markides
- Publisher
- Elsevier Science
- Year
- 1996
- Tongue
- English
- Weight
- 605 KB
- Volume
- 734
- Category
- Article
- ISSN
- 1873-3778
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📜 SIMILAR VOLUMES
## Abstract The modifications made to a flame ionization detector (FID) to facilitate the detection of large molecular weight polar compounds analyzed by capillary supercritical fluid chromatography are described. Some specific examples are given to demonstrate that polar compounds can be effective
## Abstract An on‐line coupled supercritical fluid extraction–liquid chromatography–gas chromatography–mass spectrometry (SFE‐LC‐GC‐MS) system was constructed and applied for the quantitative analysis of selected organic acids. In SFE the analytes were derivatized __in situ__ with pentafluorobenzyl
Supercritical fluid extraction (SFE) can greatly reduce the sample preparation time of analytes in solid matrices. The on-line coupling of SFE with high-speed gas chromatography (GC) can further reduce the total analysis time. SFE has been coupled to GC with a thermal desorption modulator (TDM) inte