✦ LIBER ✦
Splitless injection of large volumes of aqueous samples: Further experience. Experiments on analyzing triazines by direct injection of drinking water
✍ Scribed by Grob, Konrad ;Fröhlich, Dieter
- Publisher
- John Wiley and Sons
- Year
- 1994
- Tongue
- English
- Weight
- 363 KB
- Volume
- 17
- Category
- Article
- ISSN
- 0935-6304
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✦ Synopsis
Abstract
Conditions were optimized for the introduction of large volumes of drinking water by splitless injection with vapor overflow, experimenting with the determination of triazines. No co‐solvent was added, and the maximum injection volume was 400 μl. A vapor outlet beyond a coated precolumn was used to discharge water vapors released belatedly from the packing. Using alkali flame ionization detection (AFID), detection limits were around 0.5 μg/l.